Principles of Instrumental Analysis

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Author: Douglas A. Skoog,F. James Holler,Stanley R. Crouch

Publisher: Cengage Learning

ISBN: 1337468037

Category: Science

Page: 992

View: 6926

PRINCIPLES OF INSTRUMENTAL ANALYSIS is the standard for courses on the principles and applications of modern analytical instruments. In the 7th edition, authors Skoog, Holler, and Crouch infuse their popular text with updated techniques and several new Instrumental Analysis in Action case studies. Updated material enhances the book's proven approach, which places an emphasis on the fundamental principles of operation for each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary analog and digital electronics, computers, and the treatment of analytical data. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.

Undergraduate Instrumental Analysis, Sixth Edition

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Author: James W. Robinson,Eileen M. Skelly Frame,George M. Frame II

Publisher: CRC Press

ISBN: 9780849306501

Category: Science

Page: 1079

View: 6987

Completely rewritten, revised, and updated, this Sixth Edition reflects the latest technologies and applications in spectroscopy, mass spectrometry, and chromatography. It illustrates practices and methods specific to each major chemical analytical technique while showcasing innovations and trends currently impacting the field. Many of the chapters have been individually reviewed by teaching professors and include descriptions of the fundamental principles underlying each technique, demonstrations of the instrumentation, and new problem sets and suggested experiments appropriate to the topic. About the authors... JAMES W. ROBINSON is Professor Emeritus of Chemistry, Louisiana State University, Baton Rouge. A Fellow of the Royal Chemical Society, he is the author of over 200 professional papers and book chapters and several books including Atomic Absorption Spectroscopy and Atomic Spectroscopy. He was Executive Editor of Spectroscopy Letters and the Journal of Environmental Science and Health (both titles, Marcel Dekker, Inc.) and the Handbook of Spectroscopy and the Practical Handbook of Spectroscopy (both titles, CRC Press). He received the B.Sc. (1949), Ph.D. (1952), and D.Sc. (1978) degrees from the University of Birmingham, England. EILEEN M. SKELLY FRAME recently was Clinical Assistant Professor and Visiting Research Professor, Rensselaer Polytechnic Institute, Troy, New York. Dr. Skelly Frame has extensive practical experience in the use of instrumental analysis to characterize a wide variety of substances, from biological samples and cosmetics to high temperature superconductors, polymers, metals, and alloys. Her industrial career includes supervisory roles at GE Corporate Research and Development, Stauffer Chemical Corporate R&D, and the Research Triangle Institute. She is a member of the American Chemical Society, the Society for Applied Spectroscopy, and the American Society for Testing and Materials. Dr. Skelly Frame received the B.S. degree in chemistry from Drexel University, Philadelphia, Pennsylvania, and the Ph.D. in analytical chemistry from Louisiana State University, Baton Rouge. GEORGE M. FRAME II is Scientific Director, Chemical Biomonitoring Section of the Wadsworth Laboratory, New York State Department of Health, Albany. He has a wide range of experience in the field and has worked at the GE Corporate R&D Center, Pfizer Central Research, the U.S. Coast Guard R&D Center, the Maine Medical Center, and the USAF Biomedical Sciences Corps. He is an American Chemical Society member. Dr. Frame received the B.A. degree in chemistry from Harvard College, Cambridge, Massachusetts, and the Ph.D. degree in analytical chemistry from Rutgers University, New Brunswick, New Jersey.

Practical Instrumental Analysis

Methods, Quality Assurance and Laboratory Management

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Author: Sergio Petrozzi

Publisher: John Wiley & Sons

ISBN: 3527665919

Category: Science

Page: 492

View: 9318

This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation. What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be "fit for purpose". The book presents sixteen experiments in analytical chemistry laboratory courses. They consist of the classical curriculum used at universities and universities of applied sciences with chromatographic procedures, atom spectrometric methods, sensors and special methods (e.g. field flow fractionation , flow injection analysis and N-determination according to Kjeldahl). The carefully chosen combination of theoretical description of the methods of analysis and the detailed instructions given are what characterizes this book. The instructions to the experiments are so detailed that the measurements can, for the most part, be taken without the help of additional literature. The book is complemented with tips for effective literature and database research on the topics of organisation and the practical workflow of experiments in analytical laboratory, on the topic of the use of laboratory logs as well as on writing technical reports and grading them (Evaluation Guidelines for Laboratory Experiments). A small introduction to Quality Management, a brief glance at the history of analytical chemistry as well as a detailed appendix on the topic of safety in analytical laboratories and a short introduction to the new system of grading and marking chemicals using the "Globally Harmonized System of Classification and Labelling of Chemicals (GHS)", round off this book. This book is therefore an indispensable workbook for students, internship assistants and lecturers (in the area of chemistry, biotechnology, food technology and environmental technology) in the basic training programme of analytics at universities and universities of applied sciences.

Modern Instrumental Analysis

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Author: Satinder Ahuja,Neil Jespersen

Publisher: Elsevier

ISBN: 9780080467221

Category: Science

Page: 896

View: 7207

Modern Instrumental Analysis covers the fundamentals of instrumentation and provides a thorough review of the applications of this technique in the laboratory. It will serve as an educational tool as well as a first reference book for the practicing instrumental analyst. The text covers five major sections: 1. Overview, Sampling, Evaluation of Physical Properties, and Thermal Analysis 2. Spectroscopic Methods 3. Chromatographic Methods 4. Electrophoretic and Electrochemical Methods 5. Combination Methods, Unique Detectors, and Problem Solving Each section has a group of chapters covering important aspects of the titled subject, and each chapter includes applications that illustrate the use of the methods. The chapters also include an appropriate set of review questions. * Covers the fundamentals of instrumentation as well as key applications * Each chapter includes review questions that reinforce concepts * Serves as a quick reference and comprehensive guidebook for practitioners and students alike

A Practical Guide to Instrumental Analysis

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Author: Erno Pungor,G. Horvai

Publisher: CRC Press

ISBN: 9780849386817

Category: Science

Page: 400

View: 4651

A Practical Guide to Instrumental Analysis covers basic methods of instrumental analysis, including electroanalytical techniques, optical techniques, atomic spectroscopy, X-ray diffraction, thermoanalytical techniques, separation techniques, and flow analytical techniques. Each chapter provides a brief theoretical introduction followed by basic and special application experiments. This book is ideal for readers who need a knowledge of special techniques in order to use instrumental methods to conduct their own analytical tasks.

Instrumental analysis

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Author: Gary D. Christian,James E. O'Reilly

Publisher: Allyn & Bacon

ISBN: N.A

Category: Science

Page: 933

View: 4399

Undergraduate Instrumental Analysis, Seventh Edition

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Author: James W. Robinson,Eileen Skelly Frame,George M. Frame II

Publisher: CRC Press

ISBN: 1482233746

Category: Science

Page: 1264

View: 4749

Crucial to research in molecular biology, medicine, geology, food science, materials science, and many other fields, analytical instrumentation is used by many scientists and engineers who are not chemists. Undergraduate Instrumental Analysis, Seventh Edition provides users of analytical instrumentation with an understanding of these instruments, covering all major fields of modern instrumentation. Following the tradition of earlier editions, this text is designed for teaching undergraduates and those with no analytical chemistry background how contemporary analytical instrumentation works, as well as its uses and limitations. Each chapter provides a discussion of the fundamental principles underlying the techniques, descriptions of the instrumentation, and numerous applications. The chapters also contain updated bibliographies and problems, and most have suggested experiments appropriate to the techniques. This completely revised and updated edition covers subjects in more detail, such as a completely revised x-ray chapter, expanded coverage of electroanalytical techniques, and expansion of chromatography and mass spectrometry topics to reflect the predominance of these instruments in laboratories. This includes state-of-the-art sample introduction and mass analyzers, and the latest developments in UPLC and hyphenated techniques. The book also contains new graphics and addresses several new topics: Ion mobility spectrometry Time domain NMR (relaxometry) Electron spin resonance spectroscopy (ESR, EPR) Forensic science and bioanalytical applications Microcalorimetry and optical thermal instruments Laser-induced breakdown spectroscopy (LIBS) This text uniquely combines instrumental analysis with organic spectral interpretation (IR, NMR, and MS). It provides detailed coverage of sampling, sample handling, sample storage, and sample preparation. In addition, the authors have included many instrument manufacturers’ websites, which contain extensive resources.

Basic instrumental analysis

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Author: Burton F. Pease

Publisher: N.A

ISBN: 9780442245030

Category: Technology & Engineering

Page: 434

View: 7055

Instrumental Analysis

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Author: Robert Granger,Hank Yochum,Karl Sienerth,Jill Granger

Publisher: Oxford University Press, USA

ISBN: 9780199942312

Category:

Page: 880

View: 9602

At its core, Instrumental Analysis covers the underlying theory, instrumental design, applications, and operation of spectroscopic, electroanalytical, chromatographic, and mass spectral instrumentation. It provides students with the requisite skills to identify the comparative advantages and disadvantages in choosing one analytical technique over another by combining direct comparisons of the techniques with a discussion of how these choices affect the interpretation of the data in its final form. The text is organized into sections that include Spectroscopy & Spectrometry, Separation Science, and Electroanalytical Chemistry. Comprehensive and engaging, Instrumental Analysis provides the most modern coverage of chemical instrumentation. ABOUT THE COVER Xenon Arc lamps (sources) produce a broad spectral output from ~ 185 nm to 2000 nm. This is also the approximate spectral range of natural sunlight. Because Xenon sources can be as bright as 33,000 lumens, their relatively high intensity and broad spectral range make them well suited for UV-vis spectroscopy, where low level detection and high spectral resolution are required. This component, along with other sources such as light-emitting diodes (LEDs), is presented in chapter 6 of Instrumental Analysis.

Environmental Laboratory Exercises for Instrumental Analysis and Environmental Chemistry

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Author: Frank M. Dunnivant

Publisher: John Wiley & Sons

ISBN: 0471660272

Category: Science

Page: 416

View: 7801

A comprehensive set of real-world environmental laboratory experiments This complete summary of laboratory work presents a richly detailed set of classroom-tested experiments along with background information, safety and hazard notes, a list of chemicals and solutions needed, data collection sheets, and blank pages for compiling results and findings. This useful resource also: Focuses on environmental, i.e., "dirty" samples Stresses critical concepts like analysis techniques and documentation Includes water, air, and sediment experiments Includes an interactive software package for pollutant fate and transport modeling exercises Functions as a student portfolio of documentation abilities Offers instructors actual samples of student work for troubleshooting, notes on each procedure, and procedures for solutions preparation.

Instrumental Analysis of Intrinsically Disordered Proteins

Assessing Structure and Conformation

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Author: Vladimir Uversky,Sonia Longhi

Publisher: John Wiley & Sons

ISBN: 9780470602607

Category: Science

Page: 600

View: 7265

Instrumental techniques for analyzing intrinsically disordered proteins The recently recognized phenomenon of protein intrinsic disorder is gaining significant interest among researchers, especially as the number of proteins and protein domains that have been shown to be intrinsically disordered rapidly grows. The first reference to tackle this little-documented area, Instrumental Analysis of Intrinsically Disordered Proteins: Assessing Structure and Conformation provides researchers with a much-needed, comprehensive summary of recent achievements in the methods for structural characterization of intrinsically disordered proteins (IDPs). Chapters discuss: Assessment of IDPs in the living cell Spectroscopic techniques for the analysis of IDPs, including NMR and EPR spectroscopies, FTIR, circular dichroism, fluorescence spectroscopy, vibrational methods, and single-molecule analysis Single-molecule techniques applied to the study of IDPs Assessment of IDP size and shape Tools for the analysis of IDP conformational stability Mass spectrometry Approaches for expression and purification of IDPs With contributions from an international selection of leading researchers, Instrumental Analysis of Intrinsically Disordered Proteins: Assessing Structure and Conformation fills an important need in a rapidly growing field. It is required reading for biochemists, biophysicists, molecular biologists, geneticists, cell biologists, physiologists, and specialists in drug design and development, proteomics, and molecular medicine with an interest in proteins and peptides.

Chemical Analysis

Modern Instrumentation Methods and Techniques

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Author: Francis Rouessac,Annick Rouessac

Publisher: John Wiley & Sons

ISBN: 1118681878

Category: Science

Page: 600

View: 7312

Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail. Provides a thorough introduction to a wide range of the most important and widely used instrumental techniques Maintains a careful balance between depth and breadth of coverage Includes examples, problems and their solutions Includes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis

Contemporary Instrumental Analysis

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Author: Kenneth A. Rubinson,Judith F. Rubinson

Publisher: N.A

ISBN: 9780137907267

Category: Science

Page: 840

View: 5185

This book provides a rigorous -- yet readable -- introduction to contemporary instrumental methods of chemical analysis. It features a large number of examples of real-world applications from current journals -- showing how the principles and practices of analytical chemistry are used to produce answers to questions in all areas of scientific study and practice. KEY TOPICS: Discusses the chemistry that enhances or limits the various methods' applications and operation. Considers issues involved in sampling and sample preparation. Covers electronics and noise; electrochemical methods; spectrometry; atomic spectrometry for elemental analysis; vibrational spectrometries (infrared and Raman); nuclear magnetic resonance spectrometry; mass spectrometry; chromatography and separations; liquid chromatography; gas chromatography; electroseparations; digital signal acquisition and signal treatment; and kinetic methods. Provides numerous worked examples. For anyone interested in contemporary instrument analysis.

Methods of instrumental analysis

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Author: Instrument Society of America. Chicago Section,Instrument Society of America. Analysis Instrumentation Division

Publisher: N.A

ISBN: N.A

Category: Science

Page: N.A

View: 1363

Instrumental analysis

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Author: Charles Kenneth Mann,Thomas J. Vickers,Wilson M. Gulick

Publisher: HarperCollins Publishers

ISBN: N.A

Category: Science

Page: 766

View: 4691

Instrumental Analysis in the Biological Sciences

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Author: M. H. Gordon

Publisher: Springer Science & Business Media

ISBN: 1468415212

Category: Science

Page: 244

View: 5288

Instrumental techniques of analysis have now moved from the confines of the chemistry laboratory to form an indispensable part of the analytical armoury of many workers involved in the biological sciences. It is now quite out of the question to considcr a laboratory dealing with the analysis of biological materials that is not equipped with an extensive range of instrumentation. Recent years have also seen a dramatic improvement in the ease with which such instruments can be used, and the quality and quantity of the analytical data that they can produce. This is due in no sm all part to the ubiquitous use of microprocessors and computers for instrumental control. However, under these circumstances there is areal danger of the analyst adopting a 'black box' mentality and not treating the analytical data produced in accordance with the limitations that may be inherent in the method used. Such a problem can only be overcome if the operator is fully aware of both the theoretical and instrumental constraints relevant to the technique in question. As the complexity and sheer volume of material in undergraduate courses increases, there is a tendency to reduce the amount of fundamental material that is taught prior to embarking on the more applied aspects. This is nowhere more apparent than in the teaching of instrumental techniques of analysis.

Instrumental analysis

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Author: John H. Harley,Stephen E. Wiberley

Publisher: N.A

ISBN: N.A

Category: Chemical apparatus

Page: 440

View: 9857

index.

Proceedings

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Author: Analysis Instrumentation Symposium

Publisher: N.A

ISBN: N.A

Category: Instrumental analysis

Page: N.A

View: 9876